QEMSCAN® automated mineralogical analysis of PM2.5 and PM4: a preliminary study of underground coal mine dust from Poland and Slovenia

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dc.contributor.authorJohnson, Diane
dc.contributor.authorRollinson, Gavyn. K.
dc.contributor.authorArif, Ali Talib
dc.contributor.authorMoreno, Teresa
dc.contributor.authorTrechera Ruiz, Pedro
dc.contributor.authorLah, Robert
dc.contributor.authorLubosik, Zbigniew
dc.contributor.authorPindel, Thomas
dc.contributor.authorGminsk, Richard
dc.contributor.authorWilliamson, Ben J.
dc.date.accessioned2023-05-03T08:20:35Z
dc.date.available2023-05-03T08:20:35Z
dc.date.issued2022-09-21
dc.description.abstractDetermining the physical and chemical properties of airborne dusts in occupational settings is essential for assessing their potential toxicity as well as the effectiveness of respiratory protective equipment and dust mitigation measures. Here, we report the first successful QEMSCAN® automated mineralogical analysis of potentially toxic PM4 and PM2.5 dust from deep coal mines in Poland and Slovenia. QEMSCAN® was setup to automatically delimit 100,000 ‘particles’ per sample, based on average atomic number contrast, subject these to X-ray elemental analysis at points in a grid pattern (0.5 µm spacing), assign a mineral name to each point and then output the results as particle size, shape, mineralogy and mineral associations data and as mineral maps. The dusts were prepared as dispersions on a polyethylene sheet so that coal particles, with a slightly higher BSE signal, could be recognized from their substrate. Samples were analyzed repeatedly and in different orientations to determine the effects of sample geometry and topography. QEMSCAN® mineral identifications were manually checked using standard SEM X-ray elemental analysis. From a pilot study of Polish and Slovenian coal dust samples, PM4 and PM2.5 contain varying proportions of coal, quartz and other silicates, sulphides, sulphates, carbonates, oxides and other minerals, and notable concentrations of fly-ash particles. That some of these components may be toxic when inhaled, particularly the quartz and fly-ash, highlights the need for larger scale and wider ranging studies. The further potential of the newly developed QEMSCAN® methodology is discussed.en_UK
dc.description.sponsorshipEuropean Union funding: 754205en_UK
dc.identifier.citationJohnson D, Rollinson GK, Arif AT, et al., (2022) QEMSCAN® automated mineralogical analysis of PM2.5 and PM4: a preliminary study of underground coal mine dust from Poland and Slovenia, Frontiers in Earth Science, Volume 10, 2022, Article number 788928en_UK
dc.identifier.issn2296-6463
dc.identifier.urihttps://doi.org/10.3389/feart.2022.788928
dc.identifier.urihttps://dspace.lib.cranfield.ac.uk/handle/1826/19573
dc.language.isoenen_UK
dc.publisherFrontiersen_UK
dc.rightsAttribution 4.0 International*
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/*
dc.subjectcoal miningen_UK
dc.subjectdusten_UK
dc.subjectPM4en_UK
dc.subjectPM2.5en_UK
dc.subjectQEMSCAN®en_UK
dc.subjectautomated mineralogyen_UK
dc.titleQEMSCAN® automated mineralogical analysis of PM2.5 and PM4: a preliminary study of underground coal mine dust from Poland and Sloveniaen_UK
dc.typeArticleen_UK

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