Low hazard small-scale synthesis and chemical analysis of high purity nitroglycerine (NG)

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dc.contributor.authorContini, Alessandro E.
dc.contributor.authorFlood, Nathan
dc.contributor.authorMcAteer, Daniel
dc.contributor.authorMai, Nathalie
dc.contributor.authorAkhavan, Jacqueline
dc.date.accessioned2020-01-09T16:35:11Z
dc.date.available2020-01-09T16:35:11Z
dc.date.issued2015-10-06
dc.description.abstractA previously reported two-phase (99.5% fuming nitric acid/dichloromethane) batch method to prepare high purity 1,2,3-propanetriyl trinitrate (nitroglycerine, NG) was evaluated, simplified and adapted specifically for low hazard small-scale synthesis. The purity of the product, as determined by NMR spectroscopy, HPLC and IR spectroscopic analysis was found to be greater than 99%. The quick synthetic method is highly recommended when small amounts of highly pure NG are required for analytical and related purposes in the absence of a microreactor.en_UK
dc.identifier.citationContini AE, Flood N, McAteer D, et al., (2015) Low hazard small-scale synthesis and chemical analysis of high purity nitroglycerine (NG). RSC Advances, Volume 5, Issue 106, 2015, pp. 87228-87232en_UK
dc.identifier.cris1916629
dc.identifier.issn2046-2069
dc.identifier.urihttps:/doi.org/10.1039/C5RA17951C
dc.identifier.urihttp://dspace.lib.cranfield.ac.uk/handle/1826/14903
dc.language.isoenen_UK
dc.publisherRoyal Society of Chemistryen_UK
dc.rightsAttribution-NonCommercial 4.0 International*
dc.rights.urihttp://creativecommons.org/licenses/by-nc/4.0/*
dc.titleLow hazard small-scale synthesis and chemical analysis of high purity nitroglycerine (NG)en_UK
dc.typeArticleen_UK

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